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2-Bromo-1-(2,3-dihydro-1,4-benzodioxin-6-yl)ethan-1-one → Methyl [6-chloro-2-[(2,3-dihydro-1,4-benzodioxin-6-yl)carbonyl]-1H-indol-3-yl]acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Bromo-1-(2,3-dihydro-1,4-benzodioxin-6-yl)ethan-1-one | HCID 2776171 | — |
| 反応物 | methyl [6-chloro-2-[(5,6,7,8-tetrahydroisoquinolin-3-yl)carbonyl]-1H-indol-3-yl]acetate | HCID 9908023 | — |
| 生成物 | Methyl [6-chloro-2-[(2,3-dihydro-1,4-benzodioxin-6-yl)carbonyl]-1H-indol-3-yl]acetate | HCID 9843129 | — |
反応手順
The title compound was prepared according to the procedure described in step 2 of Example 1 from 6-bromoacetyl-2,3-dihydro-1,4-benzodioxine (J. Med. Chem. 1972, 15, 49) and methyl trans-4-chloro-2-[(phenylsulfonyl)amino]cinnamate (Example 1, step 1).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06303628B1 |
| 出典データセット | uspto-grants-2001_10 |
| ORD ID | ord-78865ab84db847f2bfe7a55d98af4855 |
| 出典メモ | uspto-grants-2001_10 |