HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-5-nitrobenzoic acid → N-(1-Adamantylmethyl)-2-chloro-5-nitrobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-5-nitrobenzoic acid | HCID 17287 | — |
| Reactant | Tricyclo(3.3.1.13,7)dec-1-ylmethylamine | HCID 86625 | — |
| Product | N-(1-Adamantylmethyl)-2-chloro-5-nitrobenzamide | HCID 584852 | 80.5% |
Reaction Steps
Prepared according to the method of Example 14 from 1-adamantanemethylamine (1.0 g) and 2-chloro-5-nitrobenzoic acid (1.22 g) to give the title compound as a yellow solid (1.7 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06303659B2 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-231ac8d8e15941248982efda6fc4c0c4 |
| Source note | uspto-grants-2001_10 |