2-Chlorobenzoyl chloride → HCID 20670013, compound

HRID 380704Notes

Reaction equation

HRID 380704 reaction equation
Cl.[Cl:2][C:3]12[CH2:12][CH:7]3[CH2:8][CH:9]([CH2:11][C:5]([CH2:13][NH2:14])([CH2:6]3)[CH2:4]1)[CH2:10]2.[Cl:15][C:16]1[CH:24]=[CH:23][CH:22]=[CH:21][C:17]=1[C:18](Cl)=[O:19]>>[Cl:15][C:16]1[CH:24]=[CH:23][CH:22]=[CH:21][C:17]=1[C:18]([NH:14][CH2:13][C:5]12[CH2:11][CH:9]3[CH2:8][CH:7]([CH2:12][C:3]([Cl:2])([CH2:10]3)[CH2:4]1)[CH2:6]2)=[O:19]

Participants

3

Reactant 2

HCID 691102-Chlorobenzoyl chlorideHCID 2836009Tricyclo[3.3.1.13,7]decane-1-methanamine, 3-chloro-, hydrochloride (1:1)

Product 1

HCID 20670013HCID 20670013, compound

Procedure

Prepared according to the method of Example 1 from 3-chloro-tricyclo[3.3.1.13,7]decane-1-methanamine, hydrochloride (0.061 g) and 2-chlorobenzoyl chloride (0.0.32 ml) to give the title compound as a white solid (0.093 g).

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-6aa86e379be84d45818b886f5f203ff8
Source dataset
uspto-grants-2001_10
Patent number
US06303659B2

Reaction notes

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