2-Methylphenyl boronic acid → HCID 21893435, compound

HRID 380995Notes

Reaction equation

HRID 380995 reaction equation
Br[C:2]1[CH:7]=[CH:6][C:5]([CH:8]([CH3:15])[CH2:9][NH:10][S:11]([CH3:14])(=[O:13])=[O:12])=[CH:4][CH:3]=1.[CH3:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=1B(O)O>O>[CH3:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=1[C:2]1[CH:7]=[CH:6][C:5]([CH:8]([CH3:15])[CH2:9][NH:10][S:11]([CH3:14])(=[O:13])=[O:12])=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 27332672-Methylphenyl boronic acidHCID 9860843HCID 9860843, compound

Product 1

HCID 21893435HCID 21893435, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The title compound was prepared from the product of Example 1 as described in Example 100 with the exception that 2-methylbenzeneboronic acid was used instead of 2-formylbenzeneboronic and 10 mL of water was added to the reaction mixture.

Workup

  1. additionwas added to the reaction mixture

Sources & evidence

ORD record
ord-a063a813890f47edb703e2bd42fa1f9a
Source dataset
uspto-grants-2001_10
Patent number
US06303816B1

Reaction notes

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