HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Salicylic Acid → Sodium Salicylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Salicylic Acid | HCID 338 | — |
| Edukt | Aniline | HCID 6115 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | Sodium | HCID 5360545 | — |
| Katalysator | Silver Nitrate | HCID 24470 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | Sodium Salicylate | HCID 16760658 | — |
Reaktionsschritte
An aqueous solution of sodium salicylate was prepared by adding 43.2 g of 2N sodium hydroxide to 12 g of salicylic acid in 240 g of demineralized water. This aqueous solution was simultaneously added with 120 mL of a 0.588 M aqueous solution of silver nitrate over a period of 10 s to 280 mL of a stirred aqueous solution containing 160 mL of a 5% aqueous solution of GAFAC ™ RM710 (an alkylphenyl- polyethene oxide-phosphate from GENERAL ANILINE), 80 mL of a 2% aqueous solution of NATRASOL™ 250L (a hydroxyethylcellulose from AQUALON) and 40 mL of demineralized water. 160 mL of a 5% aqueous solution of PIGMENTVERTEILER™ N (a sodium salt of polyacrylic acid from BASF) was then added to the resulting dispersion.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06306571B1 |
| Quelldatensatz | uspto-grants-2001_10 |
| ORD ID | ord-e866e6c6de4241159a6af5765b3c56a4 |
| Quellennotiz | uspto-grants-2001_10 |