Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thiophosgene → HCID 178424321, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thiophosgene | HCID 10040 | — |
| 반응물 | N-(4-Amino-o-tolyl)-4-chlorophthalimide | HCID 93991 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | HCID 178424321 | HCID 178424321 | 148.1% |
반응 단계
To a slurry of 150 mg (0.52 mmol) of 2-(4-amino-2-methylphenyl)-5-chlorobenzo[c]azoline-1,3-dione in 2 mL of acetone, was added 41 uL (0.54 mmol) of thiophosgene. The yellow slurry dissolved whereupon a white precipitate formed. After 1 h, this solid was collected by filtration and dried to give 127 mg (74%) of the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08524721B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-89720acaa8dc497aa652ba1ab17769eb |
| 출처 메모 | uspto-grants-2013_09 |