HuagongsheHuagongshe Chemistry Print Report · For research reference only
D-Valinol → HCID 53949057, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | D-Valinol | HCID 6950587 | — |
| Reactant | 6-[1-[3-(Isopropylamino)-2-pyridyl]piperazin-4-yl-carbonyl]nicotinic acid | HCID 18362818 | — |
| Product | HCID 53949057 | HCID 53949057 | 73% |
Reaction Steps
By the same procedure as described in the example 1, synthesis was carried out starting with 6-[1-[3-(isopropylamino)-2-pyridyl]piperazin-4-yl-carbonyl]nicotinic acid and using (R)-(−)-2-amino-3-methyl-1-butanol. Then, the product was recrystallized with acetone and hexane to give a desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06306860B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-fbe0f19cb0704256bae30c943687b702 |
| Source note | uspto-grants-2001_10 |