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HRID381369

反应详情

EQUATION

反应方程式

HRID 381369 的结构方程式

REACTANTS

反应物

2
结构：CC(C)NC(C)C
HCID7912

Diisopropylamine

C6H15N

结构：CCNc1cccnc1N1CCN(C(=O)c2ccc(C(=O)O)cn2)CC1
HCID18362847

未命名化合物

PRODUCTS

生成物

1
结构：CCNc1cccnc1N1CCN(C(=O)c2ccc(C(=O)N(C(C)C)C(C)C)cn2)CC1
HCID18362819

未命名化合物

收率 72%

PROCEDURE

实验过程

By the same procedure as described in the example 24, the synthesis was carried out starting with 6-[1-[3-(ethylamino)-2-pyridyl]piperazin-4-yl-carbonyl]nicotinic acid and using diisopropylamine. And then, the product was recrystallized with acetone and hexane to give a desired compound.

WORKUP

后处理

  1. customAnd then, the product was recrystallized with acetone and hexane