HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Methylthio)phenylhydrazine → 3-(4-Fluorophenyl)-1-(4-methylsulfinylphenyl)-4-(4-pyridyl)-5H-pyrazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Methylthio)phenylhydrazine | HCID 2760978 | — |
| Reactant | 3-(4-Fluorophenyl)-3-oxo-2-(4-pyridinyl)propanenitrile | HCID 18625655 | — |
| Reactant | 5-Amino-3-(4-fluorophenyl)-1-(methylthiophenyl)-4-(4-pyridyl)pyrazole | HCID 67635045 | — |
| Product | 3-(4-Fluorophenyl)-1-(4-methylsulfinylphenyl)-4-(4-pyridyl)-5H-pyrazole | HCID 22037500 | — |
Reaction Steps
5-Amino-3-(4-fluorophenyl)-1-(methylthiophenyl)-4-(4-pyridyl)pyrazole—The title compound is prepared following the procedure of Smith, P. A. S. et al., J. Org. Chem., 1970, 35 (7), 2215 except using 4-(methylthio)phenylhydrazine hydrochloide and 3-(4-fluorophenyl)-3-oxo-2-(pyridin-4-yl)propanenitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06306883B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-4b672a46db2d4455ba35cc03b59e2eef |
| Source note | uspto-grants-2001_10 |