Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → (E)-3-[4-(3-Dimethylaminopropenyl)phenyl]acrylic Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | (E)-3-[4-(3-dimethylaminopropenyl)phenyl]acrylic acid, methyl ester | HCID 86755260 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | (E)-3-[4-(3-Dimethylaminopropenyl)phenyl]acrylic Acid | HCID 70098974 | 85% |
반응 단계
This product was prepared by refluxing for four hours, (E)-3-[4-(3-dimethylaminopropenyl)phenyl]acrylic acid, methyl ester with NaOH (0.16 g, 2 equiv.) in 10 mL of MeOH. After evaporation of the solvent in vacuo, treatment with 5 mL of HCl (1N) gave the title compound (0.4 g, 85%) as a gummy orange solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06306870B1 |
| 출처 데이터셋 | uspto-grants-2001_10 |
| ORD ID | ord-470fc1fb6b904f5cb07de250351931b8 |
| 출처 메모 | uspto-grants-2001_10 |