HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86757514, compound → HCID 22252158, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86757514 | HCID 86757514 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22252158 | HCID 22252158 | 40% |
Reaction Steps
The same method as employed in the preparation of Example 79 but starting from a solution of (E)-(4-[3-oxo-3-(1-(3,4-methylenedioxyphenyl)-1,3,4,9-tetrahydro-β-carbolin-2-yl)propenyl]benzyloxy acetic acid, ethyl ester in EtOH gave after recrystallization from MeOH:H2O the title compound as an off-white solid in a 40% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06306870B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-93e7c8307bf647ddb286932bfdb35501 |
| Source note | uspto-grants-2001_10 |