HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stearyl Alcohol → HCID 5355041, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stearyl Alcohol | HCID 8221 | — |
| Reactant | N-Carbamylmaleimide | HCID 76868 | — |
| Product | HCID 5355041 | HCID 5355041 | 97% |
Reaction Steps
The addition of octadecanol to N-carbamylmaleimide under the conditions of Example G afforded a 97% yield of octadecyl maleurate. M.P.: 109°-11° C. (dec.); 1H NMR (CDCl3): δ10.5 (brs, 1H), 8.2 (br s, 1H), 6.3 (m, 2H), 5.4 (br s, 1H), 4.2 (t, 2H), 1.6 (m, 2H), 1.2 (m, 30H), 0.9 (t, 3H); HPLC (80% CH3CN/H2O, C18): Rt=12.8 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06307058B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-fb384a998ba948eaaac4ff53e8dffdb3 |
| Source note | uspto-grants-2001_10 |