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Phenyl isocyanate → HCID 178418499、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenyl isocyanate | HCID 7672 | — |
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | 3-(4-Phenethylpiperazin-1-yl)propanethiol dihydrochloride | HCID 13731124 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | HCID 178418499 | HCID 178418499 | 67.9% |
反応手順
The procedure described in Example 2 was followed, using 1.4 g of phenyl isocyanate, 4.0 g of 3-(4-phenethylpiperazin-1-yl)propanethiol dihydrochloride, 2.4 g of triethylamine and 50 ml of methylene chloride, to give 1.9 g (35% of theory) of N-phenyl-S-[3-(4-phenethylpiperazin-1-yl)propyl]thiocarbamate dihydrochloride monohydrate as a white crystalline solid, M.p. 272°-275° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04722926 |
| 出典データセット | uspto-grants-1988_02 |
| ORD ID | ord-5ecfcbe5ec174867b5a9332b168281de |
| 出典メモ | uspto-grants-1988_02 |