HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Tetralone → 1,2-Dihydro-4-methylnaphthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Tetralone | HCID 10724 | — |
| Reactant | HCID 178418373 | HCID 178418373 | — |
| Product | 1,2-Dihydro-4-methylnaphthalene | HCID 582327 | 68% |
Reaction Steps
α-Tetralone was reacted with methylmagnesium iodide as described in J. Org. Chem., 26, 4165 (1961), without isolation of the intermediate 1-methyl-1-tetralol, to give the desired product, after distillation, in 68% yield as a colorless oil, boiling point 55-57° C. at 0.8 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06307085B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-f467ee58ecf64abf885a0a6430418e94 |
| Source note | uspto-grants-2001_10 |