HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-benzyl-4,5-dibromopyridazin-3(2H)-one → 2-Benzyl-4-methoxy-5-bromo-3(2H)-pyridazinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-benzyl-4,5-dibromopyridazin-3(2H)-one | HCID 9902699 | — |
| Reactant | 4,5-Dibromo-2-(2,2,2-trifluoroethyl)-2,3-dihydropyridazin-3-one | HCID 16091046 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Benzyl-4-methoxy-5-bromo-3(2H)-pyridazinone | HCID 21933933 | — |
Reaction Steps
2-Benzyl-4-methoxy-5-bromo-3(2H)-pyridazinone is prepared according to the method of Example 83B starting with 2-benzyl-4,5-dibromo-3(2H)-pyridazinone, in place of 2-(2,2,2-trifluoroethyl)-4,5-dibromo-3(2H)-pyridazinone and substituting methanol in place of isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06307047B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-9ecbc7b7a9304e28901d437553efaf0e |
| Source note | uspto-grants-2001_10 |