HRID38207

反应详情

EQUATION

反应方程式

HRID 38207 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

302 mg (1.17 mmol) (RS)—S-(4-nitrophenyl)-N-(methylcarbamoyl)-S-methylsulfoximide in 20 ml methanol is hydrogenated over 60 mg palladium (10% on carbon, 50% water wet) for 4 hours at 26° C. and 30 bar. The catalyst is filtered and the solvent evaporated to give 271 mg (corresponding to 100% of theor.) of the product.

WORKUP

后处理

  1. filtrationThe catalyst is filtered
  2. customthe solvent evaporated
  3. customto give 271 mg (corresponding to 100% of theor.) of the product