HCID 10668952, compound → HCID 9873582, compound

HRID 382331Notes

Reaction equation

HRID 382331 reaction equation
[CH2:1]([C:8]1[O:9][C:10]2[CH:31]=[CH:30][CH:29]=[CH:28][C:11]=2[C:12]=1[C:13]1[CH:18]=[CH:17][C:16]([C:19]2[CH:24]=[C:23]([CH3:25])[C:22]([OH:26])=[C:21]([CH3:27])[CH:20]=2)=[CH:15][CH:14]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl[S:33]([C:36]1[CH:44]=[CH:43][C:39]([C:40]([OH:42])=[O:41])=[C:38]([OH:45])[CH:37]=1)(=[O:35])=[O:34]>>[CH2:1]([C:8]1[O:9][C:10]2[CH:31]=[CH:30][CH:29]=[CH:28][C:11]=2[C:12]=1[C:13]1[CH:14]=[CH:15][C:16]([C:19]2[CH:20]=[C:21]([CH3:27])[C:22]([O:26][S:33]([C:36]3[CH:44]=[CH:43][C:39]([C:40]([OH:42])=[O:41])=[C:38]([OH:45])[CH:37]=3)(=[O:35])=[O:34])=[C:23]([CH3:25])[CH:24]=2)=[CH:17][CH:18]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 10668952HCID 10668952, compoundHCID 146685314-(Chlorosulfonyl)-2-hydroxybenzoic acid

Product 1

HCID 9873582HCID 9873582, compound

Procedure

The title compound was prepared from 4′-(2-benzyl-benzofuran-3-yl)-3,5-dimethyl-biphenyl-4-ol and 4-chlorosulfonyl-2-hydroxy-benzoic acid, in substantially the same manner, as described in Example 1 step g, and was obtained as a white solid, mp 165-167° C.; MS m/e 603 (M−H)+;

Workup

  1. customwas obtained as a white solid, mp 165-167° C.

Sources & evidence

ORD record
ord-a4d403c42fc340d2b6743314699274c7
Source dataset
uspto-grants-2001_10
Patent number
US06310081B1

Reaction notes

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