HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → 4-Amino-1-butyl-5-imidazolecarboxamide hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | Butyl iodate | HCID 18360138 | — |
| Reactant | 4-Benzylideneamino-5-imidazolecarboxamide | HCID 53970446 | — |
| Product | 4-Amino-1-butyl-5-imidazolecarboxamide hydrochloride | HCID 18360328 | 17% |
Reaction Steps
Following the same conditions as in Reference Example 2, 14.30 g (67 mmol) of 4-benzylideneamino-5-imidazole carboxamide obtained in Reference Example 1 was reacted with butyl iodate, instead of benzyl chloride in the Reference Example 2. After the post-treatment, 2.47 g of 4-amino-1-butyl-5-imidazolecarboxamide hydrochloride was obtained (yield 17%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06310070B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-1690a845e43f49d5b906fed3ec7cf397 |
| Source note | uspto-grants-2001_10 |