HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → 4-[(Ethylamino)sulfonyl]benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | 4-(Chlorosulfonyl)benzoic acid | HCID 82385 | — |
| Product | 4-[(Ethylamino)sulfonyl]benzoic acid | HCID 611766 | 64% |
Reaction Steps
A reaction was carried out following the conditions of Example 32 using 4.4 g (20 mmol) of 4-chlorosulfonylbenzoic acid and an ethylamine solution instead of the 40% aqueous solution of methylamine. The reaction product was post-treated to obtain 2.92 g of 4-ethylaminosulfonylbenzoic acid (yield 64%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06310070B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-1d7bc9aff01a4cf78574cc20dc121891 |
| Source note | uspto-grants-2001_10 |