HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → 4-Benzyloxybenzyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | (4-(Benzyloxy)phenyl)methanol | HCID 70043 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | 4-Benzyloxybenzyl chloride | HCID 70042 | — |
Reaction Steps
A reaction and post-treatment were carried out following the conditions of Example 71 using 3 g (14 mmol) of 4-benzyloxybenzyl alcohol, 80 ml of chlorotrimethylsilane, 1.09 ml of dimethylsulfoxide, to obtain 4-benzyloxybenzyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06310070B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-5c62664dda0a49dfaeedfe28984ce662 |
| Source note | uspto-grants-2001_10 |