HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → Tert-butyl 2-(4-chloro-2-formylphenoxy)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 5-Chloro-salicylaldehyde | HCID 12481 | — |
| Reactant | tert-Butyl bromoacetate | HCID 79177 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Tert-butyl 2-(4-chloro-2-formylphenoxy)acetate | HCID 51357407 | — |
Reaction Steps
The sub-title compound was prepared by the method of Example 1 part d) using 5-chloro-2-hydroxybenzaldehyde (40 g), potassium carbonate (40 g), acetone (400 ml) and tert-butyl bromoacetate (37 ml) (yield=45.5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08524715B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-1c466732972d4d2c88e1ad16807ce345 |
| Source note | uspto-grants-2013_09 |