HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fumaric Acid → HCID 18361543, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fumaric Acid | HCID 444972 | — |
| Reactant | HCID 9823548 | HCID 9823548 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18361543 | HCID 18361543 | 41.5% |
Reaction Steps
To a solution of (−)-6-(4-biphenylyl)methoxy-2-[2-(N,N-dimethylamino)ethyl]tetralin (1.3 g) in methanol (10 ml) was added a solution of fumaric acid (0.39 g) in methanol (10 ml) and concentrated. The resulting salt was recrystallized from methanol to obtain the titled compound (0.7 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06310107B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-7d61dbc72f78416aaae9a54199aa7cdd |
| Source note | uspto-grants-2001_10 |