HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18429350, compound → HCID 18429180, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18429350 | HCID 18429350 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18429180 | HCID 18429180 | — |
Reaction Steps
1-(1,2-Dihydroxyethyl)-3,5-dinitrobenzene (0.10 g, 0.44 mmol) was dissolved in methanol (35 ml) and hydrogenation was carried out at 60 psi using a Pd/C catalyst (10%, 50 mg). The catalyst was filtered off and the solution was evaporated. Yield: 0.074 g (100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06310243B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-18c2e7ff74d44653adcb49158e78c1d4 |
| Source note | uspto-grants-2001_10 |