HuagongsheHuagongshe Chemistry Print Report · For research reference only
2486-69-3 → 4-((tert-Butoxycarbonyl)amino)-3-methoxybenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2486-69-3 | HCID 288057 | — |
| Reactant | 4-{[(Tert-butoxy)carbonyl]amino}benzoic acid | HCID 2755931 | — |
| Product | 4-((tert-Butoxycarbonyl)amino)-3-methoxybenzoic acid | HCID 15432033 | — |
Reaction Steps
4-Amino-3-methoxybenzoic acid (1 g, 5.98 mmol) was reacted according to the same procedure as that used in the process for preparing N-BOC-4-aminobenzoic acid. The resulting solid was recrystallized from ethyl acetate and hexanes to provide the desired product (1.5 g) as tan crystals: m.p. 176-178° C.;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06310095B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-36157f54cbef4f0698d56bb9a849c58e |
| Source note | uspto-grants-2001_10 |