Ammonia → HCID 18361374, compound

HRID 383137Notes

Reaction equation

HRID 383137 reaction equation
[C:1]([C:5]1[CH:10]=[CH:9][C:8]([S:11](Cl)(=[O:13])=[O:12])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].[NH3:15]>>[CH2:6]1[CH2:7][CH2:8][CH2:9][CH2:10][CH:5]1[CH2:1][CH2:2][NH:15][S:11]([C:8]1[CH:9]=[CH:10][C:5]([C:1]([CH3:4])([CH3:3])[CH3:2])=[CH:6][CH:7]=1)(=[O:13])=[O:12]

Participants

3

Reactant 2

HCID 222AmmoniaHCID 1398824-t-Butylbenzenesulfonyl chloride

Product 1

HCID 18361374HCID 18361374, compound

Procedure

The title compound was prepared according to example 1063B, replacing p-toluenesulfonyl chloride with p-tert-butylbenzenesulfonyl chloride to afford a white crystalline solid. MS (DCI/NH3) m/e 341 (M+NH4)+.

Workup

  1. customto afford a white crystalline solid

Sources & evidence

ORD record
ord-cf7068e769b24a4fb3afe8841945eacc
Source dataset
uspto-grants-2001_10
Patent number
US06310095B1

Reaction notes

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