Ammonia → HCID 18361025, compound

HRID 383140Notes

Reaction equation

HRID 383140 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][NH2:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:11]1([S:17](Cl)(=[O:19])=[O:18])[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1.N>>[CH2:3]1[CH2:4][CH2:5][CH2:6][CH:1]([CH2:7][CH2:8][CH2:9][NH:10][S:17]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)(=[O:19])=[O:18])[CH2:2]1

Participants

4

Reactant 3

HCID 222AmmoniaHCID 7369Benzenesulfonyl chlorideHCID 162593-Phenylpropylamine

Product 1

HCID 18361025HCID 18361025, compound

Procedure

The title compound was prepared according to example 1063A (replacing phenethylamine with 3-phenylpropylarnine, and example 1063B, replacing p-toluenesulfonyl chloride with benzenesulfonyl chloride to afford a colorless oil. MS (DCI/NH3) m/e 299 (M+NH4)+.

Workup

  1. customto afford a colorless oil

Sources & evidence

ORD record
ord-3498724899b0412caf9fc9dcb8ff8b09
Source dataset
uspto-grants-2001_10
Patent number
US06310095B1

Reaction notes

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