HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 25007595, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | p-Toluidine | HCID 7813 | — |
| Reactant | Phenoxodiol | HCID 219100 | — |
| Product | HCID 25007595 | HCID 25007595 | 22% |
Reaction Steps
4′,7-Dihydroxyisoflav-3-ene (499 mg, 2.08 mmol) and p-toluidine (290 mg, 2.71 mmol) were dissolved in ethanol (8 ml). Formaldehyde solution (2 ml, 0.03 mol, 37% wt) was added and the reaction stirred at room temperature for 2 days. The resulting precipitate was collected to afford the title compound (167 mg, 22%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367659B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-aefc2a68443641af869a4e1bf1d52239 |
| Source note | uspto-grants-2013_02 |