HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 25006855, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | 4-Chlorobenzylamine | HCID 66036 | — |
| Reactant | HCID 57890274 | HCID 57890274 | — |
| Product | HCID 25006855 | HCID 25006855 | 30% |
Reaction Steps
4′,7-Dihydroxy-4-(4-methoxyphenyl)isoflav-3-ene (205 mg, 0.59 mmol) was dissolved in ethanol (1 ml). 4-Chlorobenzylamine (0.09 ml, 0.74 mmol) was added followed by formaldehyde solution (0.6 ml, 8.06 mmol, 37% wt.). The reaction stirred at room temperature for 3 days. The resulting precipitate was collected to afford the title compound (90 mg, 30%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367659B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-b422acf9efb949a0836a619cefede962 |
| Source note | uspto-grants-2013_02 |