HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexyl isocyanate → HCID 178418497, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexyl isocyanate | HCID 18502 | — |
| Reactant | 3-[4-(4-Chlorophenethyl)piperazin-1-yl]propanethiol | HCID 13731125 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178418497 | HCID 178418497 | 170.7% |
Reaction Steps
The procedure described in Example 35 was followed, using 1.7 g of cyclohexyl isocyanate, 4.0 g of 3-[4-(4-chlorophenethyl)piperazin-1-yl]propanethiol and 100 ml of methylene chloride, to give 3.8 g (58% of theory) of N-cyclohexyl-S-{3-[4-(4-chlorophenethyl)piperazin-1-yl]propyl}thiocarbamate dihydrochloride as a white crystalline solid, M.p. 262°-267° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04722926 |
| Source dataset | uspto-grants-1988_02 |
| ORD ID | ord-a34cebc025d14918a8b53e7fb7577a4a |
| Source note | uspto-grants-1988_02 |