HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl iodide → HCID 68557248, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl iodide | HCID 11166 | — |
| Reactant | HCID 59233346 | HCID 59233346 | — |
| Reactant | HCID 68560033 | HCID 68560033 | — |
| Product | HCID 68557248 | HCID 68557248 | 100% |
Reaction Steps
Using tert-butyl 4-bromo-6,8,8-trimethyl-6,7,8,9-tetrahydro-[1,3]dioxolo[4,5-h]quinolin-7-one-9-carboxylate (500 mg) obtained in Example 68, 10) instead of tert-butyl 6-bromo-2,2,4-trimethyl-2,3,4,7,8,9-hexahydro-1H-cyclopenta[h]quinolin-3-one-1-carboxylate of Example 1, 8), allyl iodide instead of iodomethane of Example 1, 8) and according to a similar method, the title compound (584 mg, 100%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367695B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-ec630f2d2b564a00bc2459530118cc1c |
| Source note | uspto-grants-2013_02 |