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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 383905Generated: November 1, 2026

Allyl iodide → HCID 68557248, compound

https://huagongshe.com/reaction/383905

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAllyl iodideHCID 11166—
ReactantHCID 59233346HCID 59233346—
ReactantHCID 68560033HCID 68560033—
ProductHCID 68557248HCID 68557248100%

Reaction Steps

Using tert-butyl 4-bromo-6,8,8-trimethyl-6,7,8,9-tetrahydro-[1,3]dioxolo[4,5-h]quinolin-7-one-9-carboxylate (500 mg) obtained in Example 68, 10) instead of tert-butyl 6-bromo-2,2,4-trimethyl-2,3,4,7,8,9-hexahydro-1H-cyclopenta[h]quinolin-3-one-1-carboxylate of Example 1, 8), allyl iodide instead of iodomethane of Example 1, 8) and according to a similar method, the title compound (584 mg, 100%) was obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08367695B2
Source datasetuspto-grants-2013_02
ORD IDord-ec630f2d2b564a00bc2459530118cc1c
Source noteuspto-grants-2013_02