HCID 68428320, compound → HCID 68430732, compound

Participants

Reaction Steps

To a solution of 5-(4-(2-(3-nitrophenyl)ethoxy)phenyl)-3-isoxazolyl pivalate (100 mg) in ethyl acetate (5 ml), 13 mg of 10% palladium-carbon catalyst was added, and the reaction solution was stirred at room temperature for 1 hour under hydrogen atmosphere. The catalyst was filtered off through Celite, then the filtrate was distilled off under reduced pressure, and the residue obtained was purified by silica gel column chromatography (eluent: ethyl acetate/hexane (0:100-25:75-30:70)) to afford the title compound as a yellow oil.

Provenance & Evidence