HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 178418568, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Hexyl isocyanate | HCID 75659 | — |
| Reactant | 3-(4-Cinnamylpiperazin-1-yl)propanethiol dihydrochloride | HCID 73186836 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178418568 | HCID 178418568 | 64.2% |
Reaction Steps
The procedure described in Example 2 was followed, using 0.4 g of n-hexyl isocyanate, 1.0 g of 3-(4-cinnamylpiperazin-1-yl)propanethiol dihydrochloride, 0.6 g of triethylamine and 50 ml of methylene chloride, to give 0.44 g (31% of theory) of N-(n-hexyl)-S-[3-(4-cinnamylpiperazin-1-yl)propyl]thiocarbamate dihydrochloride as a white crystalline solid, M.p. 251°-253° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04722926 |
| Source dataset | uspto-grants-1988_02 |
| ORD ID | ord-ed77c6d5e9bf4296bf37b6996aa0f6d8 |
| Source note | uspto-grants-1988_02 |