3-Methyl-3-oxetanemethanol → HCID 68412418, compound
Reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[F:9].[CH3:10][C:11]1([CH2:15]O)[CH2:14][O:13][CH2:12]1>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][CH2:10][C:11]2([CH3:15])[CH2:14][O:13][CH2:12]2)=[CH:4][C:3]=1[F:9]Participants
3
Procedure
The title compound was prepared from 4-bromo-3-fluorophenol and (3-methyl-oxetan-3-yl)-methanol in analogy to Example 9c): MS (EI): 274 and 276 M+.
Sources & evidence
- ORD record
- ord-30bd4431f3cf400ca85ffbee2eedbbce
- Source dataset
- uspto-grants-2013_02
- Patent number
- US08367838B2
Reaction notes
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