HuagongsheHuagongshe Chemistry Print Report · For research reference only
Silane, (4-bromophenyl)trimethyl- → HCID 68409324, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Silane, (4-bromophenyl)trimethyl- | HCID 138897 | — |
| Reactant | Rac-[(3,4-dichloro-phenyl)-(methoxy-methyl-carbamoyl)-methyl]-carbamic acid tert-butyl ester | HCID 87442373 | — |
| Reactant | HCID 178418306 | HCID 178418306 | — |
| Product | HCID 68409324 | HCID 68409324 | — |
Reaction Steps
The title compound was prepared from rac-[(3,4-dichloro-phenyl)-(methoxy-methyl-carbamoyl)-methyl]-carbamic acid tert-butyl ester (Intermediate 9) and 1-bromo-4-(trimethylsilyl)benzene with tert-butyl-lithium instead of n-butyllithium in analogy to Example 1a): MS (ISP): 452.0 and 454.0 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367838B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-c4d714146e96418583489d9c67a93083 |
| Source note | uspto-grants-2013_02 |