HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentanol → Rac-[1-(4-chloro-phenyl)-2-(4-cyclopentyloxy-phenyl)-2-oxo-ethyl]-carbamic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentanol | HCID 7298 | — |
| Reactant | Rac-[1-(4-chloro-phenyl)-2-(4-hydroxy-phenyl)-2-oxo-ethyl]-carbamic acid tert-butyl ester | HCID 68409176 | — |
| Product | Rac-[1-(4-chloro-phenyl)-2-(4-cyclopentyloxy-phenyl)-2-oxo-ethyl]-carbamic acid tert-butyl ester | HCID 68411321 | — |
Reaction Steps
The title compound was prepared from rac-[1-(4-chloro-phenyl)-2-(4-hydroxy-phenyl)-2-oxo-ethyl]-carbamic acid tert-butyl ester and cyclopentanol in analogy to Example 9c): MS (ISP): 466.1 and 468.3 (M+H)+, 366.0 and 368.0 ((M-Boc)+H)+ (100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367838B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-fa1a619a063d44888a4db3dc7998a774 |
| Source note | uspto-grants-2013_02 |