HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanol → Rac-[1-(4-chloro-phenyl)-2-(4-cyclohexyloxy-phenyl)-2-oxo-ethyl]-carbamic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanol | HCID 7966 | — |
| Reactant | Rac-[1-(4-chloro-phenyl)-2-(4-hydroxy-phenyl)-2-oxo-ethyl]-carbamic acid tert-butyl ester | HCID 68409176 | — |
| Product | Rac-[1-(4-chloro-phenyl)-2-(4-cyclohexyloxy-phenyl)-2-oxo-ethyl]-carbamic acid tert-butyl ester | HCID 68408800 | — |
Reaction Steps
The title compound was prepared from rac-[1-(4-chloro-phenyl)-2-(4-hydroxy-phenyl)-2-oxo-ethyl]-carbamic acid tert-butyl ester and cyclohexanol in analogy to Example 9c): MS (ISN): 442.3 (M−H)−; MS (ISP): 444.2 (M+H)+, 344.1 ((M-Boc)+H)+ (100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367838B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-7d49faf8ba3148b3b75fa89cf5bb8061 |
| Source note | uspto-grants-2013_02 |