HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromodiphenyl Ether → Rac-[1-(3,4-dichloro-phenyl)-2-oxo-2-(4-phenoxy-phenyl)-ethyl]-carbamic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromodiphenyl Ether | HCID 7565 | — |
| Reactant | Rac-[(3,4-dichloro-phenyl)-(methoxy-methyl-carbamoyl)-methyl]-carbamic acid tert-butyl ester | HCID 87442373 | — |
| Product | Rac-[1-(3,4-dichloro-phenyl)-2-oxo-2-(4-phenoxy-phenyl)-ethyl]-carbamic acid tert-butyl ester | HCID 68408309 | — |
Reaction Steps
The title compound was prepared from rac-[(3,4-dichloro-phenyl)-(methoxy-methyl-carbamoyl)-methyl]-carbamic acid tert-butyl ester (Intermediate 9) and 1-bromo-4-phenoxy-benzene in analogy to Example 1a): MS (ISP): 472.0 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367838B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-76d7d4654522401ca7e418f93e3fc780 |
| Source note | uspto-grants-2013_02 |