HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Isopropoxybenzeneboronic acid → Rac-[1-(3,4-dichloro-phenyl)-2-(3'-isopropoxy-biphenyl-4-yl)-2-oxo-ethyl]-carbamic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Isopropoxybenzeneboronic acid | HCID 5083932 | — |
| Reactant | Rac-[1-(3,4-dichloro-phenyl)-2-(4-iodo-phenyl)-2-oxo-ethyl]-carbamic acid tert-butyl ester | HCID 68409915 | — |
| Product | Rac-[1-(3,4-dichloro-phenyl)-2-(3'-isopropoxy-biphenyl-4-yl)-2-oxo-ethyl]-carbamic acid tert-butyl ester | HCID 68408675 | — |
Reaction Steps
The title compound was prepared from rac-[1-(3,4-dichloro-phenyl)-2-(4-iodo-phenyl)-2-oxo-ethyl]-carbamic acid tert-butyl ester and 3-isopropoxyphenylboronic acid in analogy to Example 2b): MS (ISN): 512.3 and 514.3 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367838B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-fc555b2ce66d455582447e23789f4dd5 |
| Source note | uspto-grants-2013_02 |