HCID 68109218, compound → HCID 68108263, compound

Participants

Reaction Steps

3-(4-benzyloxy-3-chloro-5-methoxybenzoyl)-1,1-dioxo-2,3-dihydro-1,3-benzothiazole (519 mg) was dissolved in tetrahydrofuran (5 mL), and 20% palladium hydroxide-carbon (101 mg) was added to the solution, and then the mixture was stirred at room temperature for 21 hours under a hydrogen atmosphere. After the reaction solution was filtered, the solvent was distilled off under reduced pressure and then the obtained residue was crystallized from chloroform to obtain the title compound (185 mg) as a colorless crystal.

Provenance & Evidence