(R)-1-[4-(Benzyloxy)-3-[[(tert-butyldimethylsilyl)oxy]methyl]phenyl]-2-bromoethanol → (R)-2-Azido-1-[4-(benzyloxy)-3-[[(tert-butyldimethylsilyl)oxy]methyl]phenyl]ethanol

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	(R)-1-[4-(Benzyloxy)-3-[[(tert-butyldimethylsilyl)oxy]methyl]phenyl]-2-bromoethanol	HCID 58505102	—
Edukt	(R)-5-(2-Azido-1-((tert-butyldimethylsilyl)oxy)ethyl)-8-(benzyloxy)quinolin-2(1H)-one	HCID 58505233	—
Produkt	(R)-2-Azido-1-[4-(benzyloxy)-3-[[(tert-butyldimethylsilyl)oxy]methyl]phenyl]ethanol	HCID 58505113	—

Reaktionsschritte

The title compound was synthesized in a manner analogous to that described for Intermediate 1, using Intermediate 5 in place of (R)-8-(benzyloxy)-5-[2-bromo-1-[(tert-butyldimethylsilyl)oxy]ethyl]quinolin-2(1H)-one. ES/MS calcd. for C22H31N3NaO3Si+ 436.2. found m/z=436.2 (M+Na)+.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US08367829B2
Quelldatensatz	uspto-grants-2013_02
ORD ID	ord-e5562bdfdf2846789aa41635622ad20d
Quellennotiz	uspto-grants-2013_02