(R)-N-[5-[2-Azido-1-[(tert-butyldimethylsilyl)oxy]ethyl]-2-(benzyloxy)phenyl]formamide → N-{5-[(R)-2-amino-1-(tert-butyldimethylsilanyloxy)ethyl]-2-hydroxyphenyl}formamide

Participants

Role	Name	HCID	Charge
Reactant	(R)-N-[5-[2-Azido-1-[(tert-butyldimethylsilyl)oxy]ethyl]-2-(benzyloxy)phenyl]formamide	HCID 58505165	—
Reactant	(R)-5-(2-Amino-1-((tert-butyldimethylsilyl)oxy)ethyl)-8-hydroxyquinolin-2(1H)-one	HCID 59023604	—
Product	N-{5-[(R)-2-amino-1-(tert-butyldimethylsilanyloxy)ethyl]-2-hydroxyphenyl}formamide	HCID 57461065	—

Reaction Steps

The title compound was synthesized in a manner analogous to that described for Intermediate 2, using Intermediate 11 in place of Intermediate 1. ES/MS calcd. C15H27N2O3Si+ 311.2. found m/z=311 (M+H)+

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US08367829B2
Source dataset	uspto-grants-2013_02
ORD ID	ord-6ef909a9009044469ebd45023a74f99c
Source note	uspto-grants-2013_02