Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(R)-1-[3-Amino-4-(benzyloxy)phenyl]-2-bromoethanol → (R)-1-(3-Amino-4-(benzyloxy)phenyl)-2-azidoethanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (R)-1-[3-Amino-4-(benzyloxy)phenyl]-2-bromoethanol | HCID 11232489 | — |
| 반응물 | (R)-5-(2-Azido-1-((tert-butyldimethylsilyl)oxy)ethyl)-8-(benzyloxy)quinolin-2(1H)-one | HCID 58505233 | — |
| 생성물 | (R)-1-(3-Amino-4-(benzyloxy)phenyl)-2-azidoethanol | HCID 57516929 | — |
반응 단계
The title compound was synthesized in a manner analogous to that described for Intermediate 1, using Intermediate 13 in place of (R)-8-(benzyloxy)-5-[2-bromo-1-[(tert-butyldimethylsilyl)oxy]ethyl]quinolin-2(1H)-one. ES/MS calcd. for C15H17N4O2+ 285.1. found m/z=285 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08367829B2 |
| 출처 데이터셋 | uspto-grants-2013_02 |
| ORD ID | ord-ca1fe8518ed244528c31c3a40eed3069 |
| 출처 메모 | uspto-grants-2013_02 |