HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-6-methylpyridine → 2-(6-Bromopyridin-2-yl)-1-(tetrahydro-2H-thiopyran-4-yl)ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-6-methylpyridine | HCID 79205 | — |
| Reactant | Thiane-4-carbaldehyde | HCID 20143720 | — |
| Product | 2-(6-Bromopyridin-2-yl)-1-(tetrahydro-2H-thiopyran-4-yl)ethanol | HCID 59526031 | — |
Reaction Steps
The title compound was prepared according to the procedure in Example 158 Step 1 using 2-bromo-6-methylpyridine (1.5 g, 8.72 mmol) and tetrahydro-2H-thiopyran-4-carbaldehyde (2.27 g, 17.4 mmol) as the starting materials.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367706B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-74980b4caa884b1b9a7378aade85df60 |
| Source note | uspto-grants-2013_02 |