HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dibromopyridine → Benzyl 6-bromo-3',6'-dihydro-2,4'-bipyridine-1'(2'H)-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dibromopyridine | HCID 12274 | — |
| Reactant | 1-Carbobenzoxy-1,2,3,6-tetrahydro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine | HCID 11290836 | — |
| Product | Benzyl 6-bromo-3',6'-dihydro-2,4'-bipyridine-1'(2'H)-carboxylate | HCID 57980777 | — |
Reaction Steps
The title compound was prepared by using the procedure listed in Example 177 Step 3 with 2,6-dibromopyridine (0.77 g, 3.21 mmol) and benzyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3,6-dihydropyridine-1(2H)-carboxylate (1.05 g, 3.06 mmol) as the starting materials.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367706B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-e08bb35c072d4cb3b0a7d6b4316509ba |
| Source note | uspto-grants-2013_02 |