6-Bromopyridine-2-carbaldehyde → HCID 59526375, compound
Reaction equation
[Br:1][C:2]1[N:7]=[C:6]([CH:8]=O)[CH:5]=[CH:4][CH:3]=1.Cl.[CH:11]1([NH:16][C:17](=[O:20])[CH2:18][NH2:19])[CH2:15][CH2:14][CH2:13][CH2:12]1>>[Br:1][C:2]1[N:7]=[C:6]([CH2:8][NH:19][CH2:18][C:17]([NH:16][CH:11]2[CH2:15][CH2:14][CH2:13][CH2:12]2)=[O:20])[CH:5]=[CH:4][CH:3]=1Participants
3
Procedure
The title compound was prepared by using the procedure listed in Example 47, Step 7 with 6-bromopyridine-2-carbaldehyde (1.0 g, 5.38 mmol) and N-cyclopentylglycinamide hydrochloride (0.96 g, 5.38 mmol) as the starting materials.
Sources & evidence
- ORD record
- ord-a94ef13c6395440299ea8db6cec239ff
- Source dataset
- uspto-grants-2013_02
- Patent number
- US08367706B2
Reaction notes
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