HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 59526066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | [(2-Propanylideneamino)oxy]acetic acid | HCID 79344 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 59526066 | HCID 59526066 | — |
Reaction Steps
To {[(1-methylethylidene)amino]oxy}acetic acid (286 g, 2.18 mol) was added 600 ml of toluene. Thionyl chloride (364 g, 3.06 mol) was added dropwise at room temperature. After the addition was complete, the reaction mixture was heated to reflux for 10 hours. Toluene and thionyl chloride were evaporated under vacuum and the residue was distilled to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367706B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-10e3dbd5cef642c3a68a50a65e46166f |
| Source note | uspto-grants-2013_02 |