HRID386286

反应详情

EQUATION

反应方程式

HRID 386286 的结构方程式

PROCEDURE

实验过程

Synthesized from of 7-chloro-4-methoxy-2-phenylquinazoline (189 mg, 0.7 mmol) as 4-methyl-2-phenyl-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)quinazoline; off-white solid. MS (ES+): m/z 347.2 (20) MS (ES+): m/z 281.2 (100) [MH+-82]; HPLC: tR=3.19 min (OpenLynx, polar—5 min).

WORKUP

后处理

  1. customHPLC: tR=3.19 min (OpenLynx, polar—5 min)