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HRID38635

反应详情

EQUATION

反应方程式

HRID 38635 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc2[nH]c(-c3cccc(F)c3)cc(=O)c2c1OP(=O)(OCc1ccccc1)OCc1ccccc1
HCID49840581

未命名化合物

结构：COc1ccc2nc(-c3cccc(F)c3)cc(OP(=O)(O)O)c2c1OP(=O)(O)O
HCID56644919

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2[nH]c(-c3cccc(F)c3)cc(=O)c2c1OP(=O)(O)O
HCID49840582

未命名化合物

收率 63.7%

PROCEDURE

实验过程

Compound 51 (0.25 g, 0.46 mmol) was allowed to react in the same manner as described in the preparation of compound 49 to give 52. Yellow solid; yield: 63.7%; mp 179-181° C.; MS (ESI): m/z 366 (M+H)+; 1H-NMR (D2O+NaOD, 200 MHz): δ 3.76 (s, 3H), 6.53 (s, 1H), 7.05 (1, =8.4 Hz, 1H), 7.24-7.60 (m, 5H); Anal. (C16H13FNO6P) C, H, N.

WORKUP

后处理

  1. customto react in the same manner