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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 386351Generated: October 30, 2026

Aluminium lithium hydride → HCID 68532835, compound

https://huagongshe.com/reaction/386351

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAluminium lithium hydrideHCID 21226445—
ReactantHCID 68525508HCID 68525508—
SolventTetrahydrofuranHCID 8028—
ProductHCID 68532835HCID 6853283560%

Reaction Steps

This compound has been obtained by reacting a solution of ethyl 2-(bis(2-(3,5-bis(methoxymethyl)-1H-pyrazol-1-yl)ethyl)amino)acetate (280 mg; 0.6 mmol) in dry THF (10 mL) with LiAlH4. The title compound was isolated following the same methodology above described for the synthesis of other (hydroxymethyl)pyrazoles (see example 6). Yield: 60% (170 mg, 0.4 mmol).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08372379B2
Source datasetuspto-grants-2013_02
ORD IDord-dcab4a29dd334608bfb7c17047d9a490
Source noteuspto-grants-2013_02