Hydrochloric Acid → HCID 66845218, compound

Participants

Reaction Steps

Prepared analogously to Example 5c) starting from 2-(4-methoxyphenyl)-3-benzyloxy-6-acetamido-4H-1-benzopyran-4-one. Yield: 54%; TLC (9/1 Chloroform/Methanol) Rf: 0.60; Elem. anal. C23H19NO4*HCl; theory C, 67.40; H, 4.92; N, 3.42. found C, 64.24; H, 4.73; N, 3.20. IR (KBr): 3433, 2833, 2592, 1629, 1498, 1167 cm−1, 1H-NMR (d6-DMSO): 8.0 (m, 2H), 7.73 (m, 2H), 7.52 (dd, 1H), 7.37-7.22 (m, 5H), 7.10 (m, 2H).

Provenance & Evidence